HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methyloxybenzyl chloride → n-(3-Cyanobenzoyl)-2-[(4-methoxybenzyl)oxy]aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methyloxybenzyl chloride | HCID 69993 | — |
| Reactant | n1-(3-Cyanobenzoyl)-2-hydroxyaniline | HCID 23450340 | — |
| Reactant | Dimethylformamide potassium carbonate | HCID 86662288 | — |
| Product | n-(3-Cyanobenzoyl)-2-[(4-methoxybenzyl)oxy]aniline | HCID 23450308 | — |
Reaction Steps
Using a procedure similar to Example 32A except starting from 4-methoxybenzyl chloride and N1-(3-cyanobenzoyl)-2-hydroxyaniline and using K2CO3/DMF in place of potassium t-butoxide/THF, the title compound was obtained as a solid (27%); MS(FD): 359.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06417200B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-fdb5ce99865c4ea9a7ec481de38495e1 |
| Source note | uspto-grants-2002_07 |