HCID 9925594, compound → HCID 18470727, compound

HRID 2228603Notes

Reaction equation

HRID 2228603 reaction equation
[C:1]([C:4]1[C:8]([CH3:9])=[C:7]([C:10]2[CH:15]=[CH:14][N:13]=[CH:12][CH:11]=2)[NH:6][C:5]=1[C:16]1[CH:21]=[CH:20][N:19]=[CH:18][CH:17]=1)(=[O:3])[CH3:2].[ClH:22].CO>>[OH2:3].[ClH:22].[ClH:22].[C:1]([C:4]1[C:8]([CH3:9])=[C:7]([C:10]2[CH:11]=[CH:12][N:13]=[CH:14][CH:15]=2)[NH:6][C:5]=1[C:16]1[CH:21]=[CH:20][N:19]=[CH:18][CH:17]=1)(=[O:3])[CH3:2]

Participants

3

Reactant 2

HCID 9925594HCID 9925594, compoundHCID 21893726Hydrochloride methanol

Product 1

HCID 18470727HCID 18470727, compound

Procedure

3-Acetyl-4-methyl-2,5-di(4-pyridyl)-1H-pyrrole was dissolved in 10% HCl-MeOH. After removal of volatiles, the crude salt was recrystallized from EtOH to give the title compound.

Workup

  1. customAfter removal of volatiles
  2. customthe crude salt was recrystallized from EtOH

Sources & evidence

ORD record
ord-2cd8ffa59e4c4bb9ad6973f3e7c06232
Source dataset
uspto-grants-2002_07
Patent number
US06417202B1

Reaction notes

Loading…