HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromoaniline → (4-Bromo-phenyl)-(2-methyl-6-nitro-phenyl)-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromoaniline | HCID 7807 | — |
| Reactant | 2-Fluoro-1-methyl-3-nitrobenzene | HCID 13470957 | — |
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | (4-Bromo-phenyl)-(2-methyl-6-nitro-phenyl)-amine | HCID 68836228 | — |
Reaction Steps
The product (2.44 g) is obtained according to the method of stage 1 of Example 4, by using 1.8 g of 2-fluoro-3-methyl-nitrobenzene and 3 g of 4-bromo-aniline in the presence of 2.09 g of potassium tert-butanolate in 20 mL of DMSO.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08207373B2 |
| Source dataset | uspto-grants-2012_06 |
| ORD ID | ord-121fe60eaae74f4bb15f4c20ccd382f0 |
| Source note | uspto-grants-2012_06 |