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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2228650Generated: October 30, 2026

Potassium Iodide → HCID 15453515, compound

https://huagongshe.com/reaction/2228650

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium IodideHCID 4875—
Reactant1-Bromo-2-ChloroethaneHCID 7849—
ReactantPotassium CarbonateHCID 11430—
Reactant4'-Fluoro-2'-hydroxyacetophenoneHCID 2737326—
SolventMethyl Ethyl KetoneHCID 6569—
ProductHCID 15453515HCID 15453515—

Reaction Steps

40.5 ml of 1-bromo-2-chloroethane (490 mmol) are added at room temperature to a solution of 25 g of 1-[2-hydroxy-4-fluorophenyl]ethanone (162 mmol) in 2-butanone (400 ml), followed by addition of 45 g of potassium carbonate (320 mmol) and 1.26 g of potassium iodide (7.59 mmol).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06417222B1
Source datasetuspto-grants-2002_07
ORD IDord-cb26c966ac44430cb10139622bde5f43
Source noteuspto-grants-2002_07