3,3-Diphenylpropyl iodide → HCID 70116796, compound
Reaction equation
[SH:1][C:2]1[S:3][C:4]2[CH2:13][C:12]3[CH:11]=[C:10]([O:14][CH2:15][C:16]([O:18]CC)=[O:17])[CH:9]=[CH:8][C:7]=3[C:5]=2[N:6]=1.[C:21]1([CH:27]([C:31]2[CH:36]=[CH:35][CH:34]=[CH:33][CH:32]=2)[CH2:28][CH2:29]I)[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1>>[C:21]1([CH:27]([C:31]2[CH:32]=[CH:33][CH:34]=[CH:35][CH:36]=2)[CH2:28][CH2:29][S:1][C:2]2[S:3][C:4]3[CH2:13][C:12]4[CH:11]=[C:10]([O:14][CH2:15][C:16]([OH:18])=[O:17])[CH:9]=[CH:8][C:7]=4[C:5]=3[N:6]=2)[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1Participants
3
Procedure
Using ethyl [(2-mercapto-8H-indeno[1,2-d]thiazol-6-yl)oxy]acetate and 3,3-diphenylpropyl iodide, the procedure of Example 21 was otherwise repeated to synthesize the title compound. Yield 42%.
Sources & evidence
- ORD record
- ord-69cdcbd95502444187b0c49c3846f492
- Source dataset
- uspto-grants-2002_07
- Patent number
- US06417213B2
Reaction notes
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