3,3-Diphenylpropyl iodide → HCID 54115040, compound

HRID 2228693Notes

Reaction equation

HRID 2228693 reaction equation
[SH:1][C:2]1[S:3][C:4]2[CH2:13][C:12]3[C:11]([O:14][CH2:15][C:16]([O:18]CC)=[O:17])=[CH:10][C:9]([CH3:21])=[C:8]([CH3:22])[C:7]=3[C:5]=2[N:6]=1.[C:23]1([CH:29]([C:33]2[CH:38]=[CH:37][CH:36]=[CH:35][CH:34]=2)[CH2:30][CH2:31]I)[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1>>[C:23]1([CH:29]([C:33]2[CH:34]=[CH:35][CH:36]=[CH:37][CH:38]=2)[CH2:30][CH2:31][S:1][C:2]2[S:3][C:4]3[CH2:13][C:12]4[C:11]([O:14][CH2:15][C:16]([OH:18])=[O:17])=[CH:10][C:9]([CH3:21])=[C:8]([CH3:22])[C:7]=4[C:5]=3[N:6]=2)[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1

Participants

3

Reactant 2

HCID 155128783,3-Diphenylpropyl iodideHCID 178472966HCID 178472966, compound

Product 1

HCID 54115040HCID 54115040, compoundYield 53%

Procedure

Using ethyl [(2-mercapto-4,5-dimethyl-8H-indeno[1,2-d]thiazol-7-yl)oxy]acetate and 3,3-diphenylpropyl iodide, the procedure of Example 21 was otherwise repeated to synthesize the title compound. Yield 53%.

Sources & evidence

ORD record
ord-aa93cec6dbaa4e5e8b26f9d014113ee6
Source dataset
uspto-grants-2002_07
Patent number
US06417213B2

Reaction notes

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