HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene, 1,1'-(bromomethylene)bis(4chloro- → [(2-Bis(4-chlorophenyl)methylthio-4,5-dihydronaphtho[1,2-d]thiazol-6-yl)oxy]acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene, 1,1'-(bromomethylene)bis(4chloro- | HCID 95197 | — |
| Reactant | Ethyl[(2-mercapto-4,5-dihydronaphtho[1,2-d]thiazol-6-yl)oxy)acetate | HCID 178472952 | — |
| Product | [(2-Bis(4-chlorophenyl)methylthio-4,5-dihydronaphtho[1,2-d]thiazol-6-yl)oxy]acetic acid | HCID 18471064 | 77% |
Reaction Steps
Using ethyl [(2-mercapto-4,5-dihydronaphtho-[1,2-d]thiazol-6-yl)oxy]acetate and bis(4-chlorophenyl)methyl bromide, the procedure of Example 63 was otherwise repeated to synthesize the title compound. Yield 77%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06417213B2 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-367113eb682f4753b0477c3f2fb2e56a |
| Source note | uspto-grants-2002_07 |