Octanoic Acid → HCID 178443862, compound

HRID 2229094Notes

Reaction equation

HRID 2229094 reaction equation
[C:1]([OH:10])(=[O:9])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[CH2:11]([OH:20])[C@@H:12]([C@H:14]([C@@H:16]([CH2:18][OH:19])[OH:17])[OH:15])[OH:13].P(=O)(O)(O)O>>[C:1]([OH:10])(=[O:9])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[CH2:11]([OH:20])[C@@H:12]([C@H:14]([C@@H:16]([CH2:18][OH:19])[OH:17])[OH:15])[OH:13]

Participants

4

Reactant 3

HCID 379Octanoic AcidHCID 1004Phosphoric AcidHCID 178418489HCID 178418489, compound

Product 1

HCID 178443862HCID 178443862, compound

Conditions

Temperature
150 °C

Procedure

417.0 grams of octanoic acid was poured into a 2-liter round bottom flask with a short distillation head. A mechanical stirrer and short distillation head were attached and a heating mantle and a temperature controller was used to maintain temperature at approximately 150° C. 462.48 grams of xylitol was added slowly along with 32.422 grams of 75% phosphoric acid.

Workup

  1. customA mechanical stirrer and short distillation head were attached

Sources & evidence

ORD record
ord-d6024bc3c44243f5903e4ae6486280ad
Source dataset
uspto-grants-2002_07
Patent number
US06419941B1

Reaction notes

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