Thionyl Chloride → HCID 18431210, compound
Reaction equation
[O:1]([CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][C:18]([OH:20])=O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.S(Cl)([Cl:23])=O>>[O:1]([CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][C:18]([Cl:23])=[O:20])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1Participants
3
Procedure
250 mg of 11-phenoxy undecanoic acid (commercial) is mixed with 2 ml of pure thionyl chloride and the whole is left overnight at ambient temperature. In this way 265 mg of expected product is obtained.
Sources & evidence
- ORD record
- ord-76068dee1b2945b3a41d40c2ded0db76
- Source dataset
- uspto-grants-2002_07
- Patent number
- US06420341B1
Reaction notes
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