Bromotrimethylsilane → HCID 11013760, compound

Participants

Reaction Steps

A suspension in acetonitrile of 235 mg (0.567 mmol) of the compound obtained in Example 29 and 0.75 ml (5.67 mmol) of bromotrimethylsilane is heated for 1 hour 30 minutes at reflux of the acetonitrile (3 ml). Evaporation to dryness is carried out, the residue is taken up in methanol, and the solution is stirred for 30 minutes and then evaporated to dryness again. The residue is triturated in acetonitrile and the precipitate corresponding to the title product is filtered off.

Provenance & Evidence