Thionyl Chloride → HCID 70158102, compound

Participants

Reaction Steps

Thionyl chloride (5.0 ml) was added to a solution of (E)-3-(2-naphthyl)-2-buten-1-ol (4.59 g) in CH2Cl2 (30 ml)at 0° C. and the mixture was refluxed for 4 hours. The mixture was washed with water, saturated NaHCO3 solution and brine, dried and concentrated. The residue was washed with hexane to give the titled compound (1.22 g) as a white solid.

Provenance & Evidence