HCID 16105572, compound → HCID 16105581, compound

Participants

Reaction Conditions

Reaction Steps

A solution of diisobutylaluminum hydride in toluene (1.5M, 25 ml) was added dropwise to a solution of ethyl (E)-3-(5,6,7,8-tetrahydro-2-naphtyl)crotonate (3.72 g) in CH2Cl2 at −78° C. and the mixture was stirred at −78° C. for 15 minutes. The reaction mixture was washed with 1N HCl and brine, dried and concentrated to give the titled compound (2.65 g) as a colorless oil.

Provenance & Evidence