Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 2-Aminothiophenol | HCID 8713 | — |
| Reactant | Azlactone | HCID 65073 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 117998-90-0 | HCID 14065320 | — |
Reaction Steps
2-Aminothiophenol (1.2 ml) is added to a solution of 2-phenyl-4,5-dihydro-1,3-oxazol-5-one (1.8 g) in acetic acid (14 ml), and the mixture is stirred for one hour while heating it at 40° C. Water is added to the reaction mixture, and the resulting precipitate is filtered off to give 2-(benzoylaminomethyl)benzothiazole (0.75 g) as crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06420398B2 |
|---|
| Source dataset | uspto-grants-2002_07 |
|---|
| ORD ID | ord-18a0df3084f24dd093a856c531ab155b |
|---|
| Source note | uspto-grants-2002_07 |
|---|
