HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 178418706, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Ethyl 3-[({3'-[(aminocarbothioyl)amino][1,1'-biphenyl]-3-yl}sulfonyl)-amino]-3-phenylpropanoate | HCID 21982442 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178418706 | HCID 178418706 | — |
Reaction Steps
2.42 g of Ethyl 3-[({3′-[(aminocarbothioyl)amino][1,1′-biphenyl]-3-yl}sulfonyl)-amino]-3-phenylpropanoate 14.1.1 were dissolved in 80 ml methanol and 0.89 g Iodomethan were added. After reflux for 2 h, the reaction mixture was concentrated and crystalized from ether to obtain 3.1 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06420396B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-56a4a91885af4801b4ec7faf7f4e72b0 |
| Source note | uspto-grants-2002_07 |