HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 12966957, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 12966956 | HCID 12966956 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 12966957 | HCID 12966957 | — |
Reaction Steps
The tetrahydropyranyl ether (5) (5.03 9) was dissolved into a dry methanol (300 ml), into which potassium carbonate (1.49 g ) was added, and stirred at room temperature for 6 hours. A crude compound obtained by a usual work-up was column-chromatographed to give the title compound (6). Yield: 3.25 g
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06420422B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-5b163ac341b5476f9757f9a94c825b31 |
| Source note | uspto-grants-2002_07 |