HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisobutylaluminum hydride → HCID 12966958, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisobutylaluminum hydride | HCID 14487 | — |
| Reactant | HCID 12966957 | HCID 12966957 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 12966958 | HCID 12966958 | — |
Reaction Steps
Alcohol (6) (2.00 g) was reduced in dry toluene (40 ml) using DIBAL-H at −70° C. The lactol (7) was obtained by a usual work up.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06420422B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-b045ea7e5d3946cca60f1c7f02ea45bc |
| Source note | uspto-grants-2002_07 |