HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorine → HCID 18469461, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorine | HCID 24526 | — |
| Reactant | 3,5-Dimethylbenzoyl Chloride | HCID 81088 | — |
| Catalyst | Iron chloride (FeCl3) | HCID 24380 | — |
| Product | HCID 18469461 | HCID 18469461 | 64.8% |
Reaction Steps
A stirred apparatus with gas feed and discharge to an eliminator was initially charged with 100 g (0.593 mol) of 3,5-dimethylbenzoyl chloride together with 0.5 g of iron (III) chloride, and 42 g of chlorine were introduced at 22-28° C. over the course of 3 hours. Fractional distillation gave 78 g of 2-chloro-3,5-dimethylbenzoyl chloride. Boiling range: 113-114° C. at 5 mbar.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06420601B2 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-d46adb34f87b4960a909ce4e598f9403 |
| Source note | uspto-grants-2002_07 |