HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Nitrophenylboronic Acid → HCID 9903502, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Nitrophenylboronic Acid | HCID 1677 | — |
| Reactant | 6-Bromo-1-methyl-1H-benzo(d)imidazol-2(3H)-one | HCID 9815982 | — |
| Product | HCID 9903502 | HCID 9903502 | — |
Reaction Steps
Prepared from 1-methyl-6-bromo-1,3-dihydro-benzoimidazol-2-one and 3-nitro-phenyl boronic acid in the same fashion as that of Example 5. White solid: mp 264-265° C.; 1H-NMR (DMSO-d6) δ 11.0 (s, 1H), 8.47 (t, 1H, J=1.5 Hz), 8.19-8.15 (m, 2H), 7.75 (t, 1H, J=8.25 Hz), 7.58 (d, 1H, J=1.5 Hz), 7.43 (dd, 1H, J=8.25, 1.5 Hz), 7.1 (d, 1H, J=8.25 Hz), 3.37 (s, 3H); MS (ES) m/z 268([M−H]−, 50%); Anal. Calc. For C14H11N3O3: C, 62.45, H, 4.12, N, 15.61. Found: C, 61.48, H, 4.36 N, 14.75.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06423699B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-3d126c42351a4d7b8fb2916431a0baaf |
| Source note | uspto-grants-2002_07 |