HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Nitroaniline → HCID 18180124, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Nitroaniline | HCID 7423 | — |
| Reactant | 5-Chloro-3-methylbenzo(b)thiophene-2-sulfonyl chloride | HCID 2735756 | — |
| Reactant | HCID 18180123 | HCID 18180123 | — |
| Product | HCID 18180124 | HCID 18180124 | — |
Reaction Steps
The title compound (E123) was prepared from 6-(4-methylpiperazin-1-yl)-2,3-dihydro-1H-indole (prepared from 3-nitroaniline, using methodology of WO95/06637 Intermediate 3) (39 mg, 0.18 mmol) and 5-chloro-3-methylbenzo[b]thiophene-2-sulfonyl chloride (50 mg; 0.18 mmol) using the method of Example 1 (75 mg, 84%) MH+=462/464.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06423717B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-72d604cdf885482d8d60b7ef80875096 |
| Source note | uspto-grants-2002_07 |