HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-4-nitrobenzoic acid → HCID 18465930, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-4-nitrobenzoic acid | HCID 7448 | — |
| Reactant | Methyl isocyanoacetate | HCID 547815 | — |
| Product | HCID 18465930 | HCID 18465930 | — |
Reaction Steps
The procedures of Example 1-(l) were followed, except for replacing the 2-methoxy-4-nitrobenzoic acid with 18.1 g (0.09 g) of 2-chloro-4-nitrobenzoic acid and replacing the ethyl isocyanoacetate with 9.9 g (0.1 mol) of methyl isocyanoacetate, to give 16.2 g (0.057 mol, 63.7% based on the 2-chloro-4-nitrobenzoic acid) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06423849B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-100dd10ae17942929e5edb34bfcc2418 |
| Source note | uspto-grants-2002_07 |