HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → 3-(Diethoxymethylsilyl)propylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | (3-Chloropropyl)diethoxymethylsilane | HCID 83536 | — |
| Product | 3-(Diethoxymethylsilyl)propylamine | HCID 18511 | — |
Reaction Steps
According to Example 1, 6.6 kg (31.1 mol) 3-chloropropylmethyldiethoxysilane are reacted with 24 kg (1412 mol) ammonia, excess ammonia is removed by pressure distillation and flash processes and the 3-aminopropylmethyldiethoxysilane that is formed is isolated by filtration and vacuum distillation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06423858B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-8f2d3ec8a5a147e095b0afe21429f272 |
| Source note | uspto-grants-2002_07 |