HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 56609623, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 57313411 | HCID 57313411 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 56609623 | HCID 56609623 | — |
Reaction Steps
was synthesized from 600b by methods similar to those used to make 602n from 600b, using the reagent obtained from reacting DMF with 3 equiv. of oxalyl chloride in a CH2Cl2 solution as R3X, to afford 404 mg of 652.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06423840B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-fa98d2bd0ad742f7b5ebb3e1bd57cc6c |
| Source note | uspto-grants-2002_07 |