HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18464911, compound → HCID 18464760, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18464911 | HCID 18464911 | — |
| Reactant | 4-(1-(2-ethoxyethyl)-1H-benzimidazol-2-yl) [1,4]diazepane hydriodic acid salt | HCID 86583887 | — |
| Product | HCID 18464760 | HCID 18464760 | — |
Reaction Steps
Prepare by the method of Example 7.6 using 1-(2,4,5-trimethoxybenzoyl)-3-phenyl-3-(2-methanesulfonyloxyethyl) pyrrolidine and 4-(1-(2-ethoxyethyl)-1H-benzimidazol-2-yl)[1,4]diazepane hydriodic acid salt to give the title compound: Rf=0.42 (silica gel, 9/1/0/1 dichloromethane/methanol/concentrated aqueous ammonia).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06423704B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-0da9e83bfb96469ea8fd6a9154d1fd20 |
| Source note | uspto-grants-2002_07 |