Bismuth-oxygen → HCID 69984439, compound

Participants

Reaction Steps

The benzil compound was synthesized according to the procedure of Example 41, Step 3 using the product of Step 1 (3.5 g, 12 mmol) and bismuth oxide (6.6 g, 14 mmol) in acetic acid (35 ml). There was obtained 2.8 g (85%) of the desired benzil as a-crystalline solid: mp 152-154° C. Anal. Calc'd. for C15H10FClO3 (MW .292.70): C, 61.55; H, 3.44. Found: C, 61.40; H, 3.31.

Provenance & Evidence