HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropylamine → HCID 13885084, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropylamine | HCID 6363 | — |
| Reactant | Acetic acid, 2-chloro-2-fluoro-, ethyl ester | HCID 101668 | — |
| Catalyst | Ethylene Glycol | HCID 174 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13885084 | HCID 13885084 | — |
Reaction Steps
A solution of 11.8 grams (0.2 mole) isopropyl amine in 20 milliliters ethyl alcohol were added dropwise at 10°-15° C. with stirring to a solution of ethyl fluorochloroacetate and 5 drops of ethylene glycol in 80 milliliters ethyl alcohol. The solution was stirred at 10°-20° C. for 2 hours and was then stored at -15° C. for 3 days. At this time, the solution was evaporated to leave a liquid, 25.2 grams, nD30 1.4395, identified as the title compound by infrared and nuclear magnetic resonance spectroscopy.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04781752 |
| Source dataset | uspto-grants-1988_11 |
| ORD ID | ord-9135bc465a944c0a96fcc19a20b15fa1 |
| Source note | uspto-grants-1988_11 |