HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon Dioxide → HCID 21286380, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon Dioxide | HCID 280 | — |
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | HCID 10397985 | HCID 10397985 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21286380 | HCID 21286380 | — |
Reaction Steps
To nitric acid (density=1.50) cooled with dry ice and methanol is added 1,2,3,4-tetrahydro-1-oxo-2-naphthaleneacetic acid at -10 to -15° C. The resulting mixture is stirred below 0° C. for 40 minutes and poured into ice. The precipitated crystals are collected by filtration to give 7-nitro-1,2,3,4-tetrahydro-1-oxo-2-naphthaleneacetic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04782057 |
| Source dataset | uspto-grants-1988_11 |
| ORD ID | ord-dea452f5407b470c90d9b63e727d76ac |
| Source note | uspto-grants-1988_11 |