Benzyl Bromide → HCID 67931549, compound

Participants

Reaction Steps

A solution of 2,2'-(3,5,5-trimethylhexylidene)-bis(4,6-dimethylphenol) (184.0 g, 0.5 mole) in acetone (21) was stirred with anhydrous potassium carbonate (170 g) and benzylbromide (85.5 g, 0.5 mole) at room temperature overnight. The solution was filtered, excess acetone removed under vacuum and the residue refrigerated. The crystalline solid was filtered off, washed with cold acetone and dried under vacuum at 40° C. Yield=66%. M.p.=125°-126° C.

Provenance & Evidence