HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Naphthalenediamine → HCID 178432073, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Naphthalenediamine | HCID 13648 | — |
| Reactant | Triethyl orthoacetate | HCID 66221 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178432073 | HCID 178432073 | — |
Reaction Steps
To a solution of 7.38 g of 1,2-diaminonaphthalene in 175 ml of ethanol was added 8.56 ml of triethyl orthoacetate and the reaction mixture heated to reflux for 3.5 hours. The solvent was removed in vacuo and the residue partitioned between chloroform and water. The organic phase was separated, dried over magnesium sulfate and concentrated to a dark oil, 9.0 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04782050 |
| Source dataset | uspto-grants-1988_11 |
| ORD ID | ord-6865c7ab614b466c9be70ca655209577 |
| Source note | uspto-grants-1988_11 |