HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → 1-Methyl-5-phenylimidazole-2-carboxaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | 1-Methyl-5-phenyl-1H-imidazole | HCID 3746343 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Product | 1-Methyl-5-phenylimidazole-2-carboxaldehyde | HCID 22493878 | — |
Reaction Steps
Using the procedure of Example 1D, 640 mg of 1-methyl-5-phenylimidazole, 1.55 ml of 2.6M n-butyllithium and 0.31 ml of dimethylformamide gave 320 mg of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04782050 |
| Source dataset | uspto-grants-1988_11 |
| ORD ID | ord-1f3c8e83675c4d4badac458933e88fa7 |
| Source note | uspto-grants-1988_11 |