Triethylorthoaceate → HCID 21286293, compound

HRID 2231265Notes

Reaction equation

HRID 2231265 reaction equation
N#N.[CH3:3][NH:4][C:5]1[C:10]([F:11])=[CH:9][CH:8]=[CH:7][C:6]=1[NH2:12].[CH2:13](C(CC)(CC)C([O-])([O-])[O-])[CH3:14]>C(O)C>[CH3:3][N:4]1[C:5]2[C:10]([F:11])=[CH:9][CH:8]=[CH:7][C:6]=2[N:12]=[C:13]1[CH3:14]

Participants

4

Reactant 2

HCID 21875354TriethylorthoaceateHCID 86742506HCID 86742506, compound

Product 1

HCID 21286293HCID 21286293, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Following the procedure of Preparation O-1, 3.0 g of N2 -methyl-3-fluorophenylenediamine and 3.9 ml of triethylorthoacetate in 100 ml of ethanol gave 3.0 g of product.

Sources & evidence

ORD record
ord-39c8473989cc4f2cb9aea68d53d60eca
Source dataset
uspto-grants-1988_11
Patent number
US04782050

Reaction notes

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