HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1'-Carbonyldiimidazole → 1-Methyl-5-imidazolyl carboxylic acid imidazolide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | 1-methyl-1H-imidazole-5-carboxylic acid | HCID 2773507 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 1-Methyl-5-imidazolyl carboxylic acid imidazolide | HCID 86739967 | — |
Reaction Steps
1-methyl-5-imidazole carboxylic acid, 7.0 gm, was added to 50 ml of methylene chloride. 5.2 gm of carbonyldiimidazole was added to the system. The system was stirred at room temperature for 18 hours to give the 1-methyl-5-imidazolyl carboxylic acid imidazolide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04782074 |
| Source dataset | uspto-grants-1988_11 |
| ORD ID | ord-8de8efd20bb0459d8e78ca48276b3325 |
| Source note | uspto-grants-1988_11 |