참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | 3-(2,4-Dichlorophenyl)-3-oxopropanenitrile | HCID 13630728 | — |
| 생성물 | 2-(2,4-Dichloro-benzoyl)-3-methoxyacrylonitrile | HCID 53739244 | 104.5% |
반응 단계
A mixture of 8.8 g of 2,4-dichloro-benzoylacetonitrile, 69.2 g of methyl o-formate and 10.5 g of acetic anhydride is refluxed at a bath temperature of 150° C. for 3 hours. The volatile constituents are then distilled off in vacuo and finally under a fine vacuum at a bath temperature of 120° C. 11 g of 2-(2,4-dichloro-benzoyl)-3-methoxy-acrylonitrile are obtained as a viscous oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04782156 |
|---|
| 출처 데이터셋 | uspto-grants-1988_11 |
|---|
| ORD ID | ord-e82b55d05cf543499e6b7f9ea7ecd2c5 |
|---|
| 출처 메모 | uspto-grants-1988_11 |
|---|
