HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178521058, compound → HCID 53633108, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178521058 | HCID 178521058 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 53633108 | HCID 53633108 | — |
Reaction Steps
A mixture of 5 g of 7-β-D-arabinofuranosyl-3,7-dihydro-4H-pyrrolo[2,3-d]pyrimidine-4-thione, 5 g of Raney nickel, and 250 ml of water is stirred and heated under reflux for one hour and filtered while hot. The filtrate is evaporated in vacuo to a small volume and cooled to provide pure 7-β-D-arabinofuranosyl-7H-pyrrolo[2,3-d]pyrimidine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04352795 |
| Source dataset | uspto-grants-1982_10 |
| ORD ID | ord-11c2662a241b44a0a3c6f466c67ac935 |
| Source note | uspto-grants-1982_10 |