HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 21273113, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | HCID 21273105 | HCID 21273105 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 21273113 | HCID 21273113 | — |
Reaction Steps
A mixture of 7.2 g of 2-nonylbenzyl bromide, 5.77 g of triphenylphosphine and 60 ml of toluene is heated under reflux for 4 hours, cooled and diluted with 80 ml of ether. The 2-nonylbenzyltriphenylphosphonium bromide that separates out is removed by filtration, washed with ether and dried in vacuo; m.p. 174°-176°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04785004 |
| Source dataset | uspto-grants-1988_11 |
| ORD ID | ord-5b939655320c4c63a9e5fe5d505021ee |
| Source note | uspto-grants-1988_11 |