HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 4714992, compound → HCID 14324234, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 4714992 | HCID 4714992 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | 1-Propanol | HCID 1031 | — |
| Product | HCID 14324234 | HCID 14324234 | 60% |
Reaction Steps
Then 243 parts of 2,5-dimethyl-8-methoxyquinoline in 0.6 l propanol and 20 parts Raney nickel were hydrogenated at 80° C. under 6.9 MPa for 4 hours. This was filtered and solvent stripped under reduced pressure and distilled in vacuum to yield 60% of 2,5-dimethyl-8-methoxy-1,2,3,4-tetrahydroquinoline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04788121 |
| Source dataset | uspto-grants-1988_11 |
| ORD ID | ord-b8b869f82c934f49b6e232b03ec9d547 |
| Source note | uspto-grants-1988_11 |