HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → [2-(Nitrophenyl)ethenyl]diazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Pyridazine | HCID 9259 | — |
| Reactant | Pyrimidine | HCID 9260 | — |
| Reactant | Pyrazine | HCID 9261 | — |
| Reactant | 2-Nitrobenzaldehyde | HCID 11101 | — |
| Reactant | 3-Methylpyridazine | HCID 74208 | — |
| Solvent | Formic Acid | HCID 284 | — |
| Product | [2-(Nitrophenyl)ethenyl]diazine | HCID 70378905 | — |
Reaction Steps
Reaction of a nitrobenzaldehyde (III) with a methyldiazine [pyrimidine (IVA), pyrazine (IVB) or pyridazine (IVC)]in a suitable solvent such as acetic anhydride, formic acid or the like to produce a corresponding [2-(nitrophenyl)ethenyl]diazine (VA, VB or VC) pursuant to the following reaction scheme: ##STR7##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04788198 |
| Source dataset | uspto-grants-1988_11 |
| ORD ID | ord-471bd072f89d4098984c5e11472a668c |
| Source note | uspto-grants-1988_11 |