HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Trifluoromethyl)benzoyl chloride → ethyl N-(o-trifluoromethyl-benzoyl)-o-methoxybenzimidate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Trifluoromethyl)benzoyl chloride | HCID 67561 | — |
| Reactant | Ethyl o-methoxybenzimidate | HCID 11252328 | — |
| Product | ethyl N-(o-trifluoromethyl-benzoyl)-o-methoxybenzimidate | HCID 21283805 | — |
Reaction Steps
starting from ethyl o-methoxybenzimidate and o-trifluoromethyl-benzoyl chloride there is obtained ethyl N-(o-trifluoromethyl-benzoyl)-o-methoxybenzimidate and therefrom with methylhydrazine there is obtained 3-(o-anisyl)-1-methyl-5-(o-trifluoromethyl-phenyl)-1H-1,2,4-triazole, m.p. 74°-78° C.;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04788210 |
| Source dataset | uspto-grants-1988_11 |
| ORD ID | ord-bcebb518d8be4666b4fb987f90325460 |
| Source note | uspto-grants-1988_11 |