HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Trifluoromethyl)benzoyl chloride → ethyl N-(o-trifluoromethyl-benzoyl)-2-fluoro-4-chlorobenzimidate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Trifluoromethyl)benzoyl chloride | HCID 67561 | — |
| Reactant | Ethyl 4-chloro-2-fluorobenzimidate | HCID 19373098 | — |
| Product | ethyl N-(o-trifluoromethyl-benzoyl)-2-fluoro-4-chlorobenzimidate | HCID 21283811 | — |
Reaction Steps
starting from ethyl 4-chloro-2-fluorobenzimidate and o-trifluoromethyl-benzoyl chloride there is obtained ethyl N-(o-trifluoromethyl-benzoyl)-2-fluoro-4-chlorobenzimidate and therefrom with methylhydrazine there is obtained 3-(4-chloro-2-fluorophenyl)-1-methyl-5-(o-trifluoromethyl-phenyl)-1H-1,2,4-triazole, m.p. 109.5°-112° C.;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04788210 |
| Source dataset | uspto-grants-1988_11 |
| ORD ID | ord-3daaab40184244b4bb87d50d9da2fd6c |
| Source note | uspto-grants-1988_11 |