2-Iodobenzamide → HCID 10901813, compound

HRID 2232457Notes

Reaction equation

[I:1][C:2]1[CH:10]=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([NH2:6])=[O:5].F[B-](F)(F)F.[CH2:16]([O+](CC)CC)[CH3:17]>>[I:1][C:2]1[CH:10]=[CH:9][CH:8]=[CH:7][C:3]=1[C:4](=[NH:6])[O:5][CH2:16][CH3:17]

Participants

Reactant 2

HCID 775292-Iodobenzamide

HCID 2723982Triethyloxonium tetrafluoroborate

Product 1

HCID 10901813HCID 10901813, compound

Procedure

starting from o-iodobenzamide and triethyloxonium tetrafluoroborate there is obtained ethyl o-iodobenzimidate as an oil; 1H-NMR(CDCl3): 1.42 (t, CH3), 4.38 (q, CH2), 6.8-7.6 (3 aromatic H+NH), 7.8-8.05 (1 aromatic H);

Sources & evidence

ORD record: ord-6ffeaa83c55d436ebbd7281b7586fb04
Source dataset: uspto-grants-1988_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04788210

Reaction notes

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