3-Chloro-2-fluorobenzamide → HCID 21283785, compound

HRID 2232458Notes

Reaction equation

[Cl:1][C:2]1[C:3]([F:11])=[C:4]([CH:8]=[CH:9][CH:10]=1)[C:5]([NH2:7])=[O:6].F[B-](F)(F)F.[CH2:17]([O+](CC)CC)[CH3:18]>>[Cl:1][C:2]1[C:3]([F:11])=[C:4]([CH:8]=[CH:9][CH:10]=1)[C:5](=[NH:7])[O:6][CH2:17][CH3:18]

Participants

Reactant 2

HCID 5178423-Chloro-2-fluorobenzamide

HCID 2723982Triethyloxonium tetrafluoroborate

Product 1

HCID 21283785HCID 21283785, compound

Procedure

starting from 3-chloro-2-fluorobenzamide and triethyloxonium tetrafluoroborate there is obtained ethyl 3-chloro-2-fluorobenzimidate as an oil; mass spectrum: 200 (10), 173 (25), 166 (15), 157 (100), 156 (73);

Sources & evidence

ORD record: ord-ba8f3a36fb2143bbba50828c8cc7094e
Source dataset: uspto-grants-1988_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04788210

Reaction notes

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