Triethyloxonium tetrafluoroborate → HCID 21283788, compound

HRID 2232459Notes

Reaction equation

[Cl:1][C:2]1[C:10]([Cl:11])=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([NH2:6])=[O:5].F[B-](F)(F)F.[CH2:17]([O+](CC)CC)[CH3:18]>>[Cl:1][C:2]1[C:10]([Cl:11])=[CH:9][CH:8]=[CH:7][C:3]=1[C:4](=[NH:6])[O:5][CH2:17][CH3:18]

Participants

Reactant 2

HCID 2723982Triethyloxonium tetrafluoroborate

HCID 27359562,3-Dichlorobenzamide

Product 1

HCID 21283788HCID 21283788, compound

Procedure

starting from 2,3-dichlorobenzamide and triethyloxonium tetrafluoroborate there is obtained ethyl 2,3-dichlorobenzimidate as an oil; mass spectrum: 216 (16), 189 (20), 182 (9), 173 (100), 172 (56);

Sources & evidence

ORD record: ord-f5cc4f1b17d34c55ac37d10b1a975dd9
Source dataset: uspto-grants-1988_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04788210

Reaction notes

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