HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 13769181, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 1-Piperidinecarbonyl chloride | HCID 242085 | — |
| Reactant | HCID 178515531 | HCID 178515531 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 13769181 | HCID 13769181 | 13.7% |
Reaction Steps
The procedure is as in Example 33, but starting with 4-phenyl-2-quinolinol (2.47 g), triethylamine (2.33 cc) and 1-(chlorocarbonyl)piperidine (2.47 g) in dimethylformamide (30 cc). The residue obtained is purified by chromatography on silica gel using a cyclohexane/ethyl acetate (80:20 by volume) eluant. 4-Phenyl-2-quinolyl 1-piperidinecarboxylate (0.51 g), m.p. 85° C., is thereby isolated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04788199 |
| Source dataset | uspto-grants-1988_11 |
| ORD ID | ord-4f0a05bccc744d5fa3d93ac79cff9478 |
| Source note | uspto-grants-1988_11 |