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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 2232537생성일: 2026년 10월 26일

Ethyl 2-(3-methoxyphenyl)-4-quinazolinepropionate → N,N-diethyl-2-(3-methoxyphenyl)-4-quinazolinepropanamide

https://huagongshe.com/reaction/2232537

반응식

참여 물질

역할이름HCID투입량
반응물Ethyl 2-(3-methoxyphenyl)-4-quinazolinepropionateHCID 13769245—
용매DiethylamineHCID 8021—
생성물N,N-diethyl-2-(3-methoxyphenyl)-4-quinazolinepropanamideHCID 1376915655.5%

반응 단계

The procedure is as in Example 1, starting with ethyl 2-(3-methoxyphenyl)-4-quinazolinepropionate (1.2 g) and diethylamine (30 cc). After chromatography on silica gel with a cyclohexane/ethyl acetate (1:1 by volume) mixture as eluant, and crystallization in isopropyl ether, N,N-diethyl-2-(3-methoxyphenyl)-4-quinazolinepropanamide (0.36 g), m.p. 87° C., is obtained.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04788204
출처 데이터셋uspto-grants-1988_11
ORD IDord-899babe8936a487ba126e7d4fda9b679
출처 메모uspto-grants-1988_11