HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Mercaptopropionic Acid → HCID 21283574, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Mercaptopropionic Acid | HCID 6514 | — |
| Reactant | 4-chloro-2-phenylquinoline | HCID 278376 | — |
| Reactant | HCID 408483 | HCID 408483 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 21283574 | HCID 21283574 | 54.9% |
Reaction Steps
4-Chloro-2-phenylquinoline (4.8 g) and 3-mercaptopropionic acid (2.54 g) in pyridine (50 cc) are heated under reflux for 11 hours. After a treatment similar to that described in Example 54 for 2-[(2-phenyl-4-quinolyl)thio]acetic acid, 3-[(2-phenyl-4-quinolyl)thio]propionic acid (3.4 g) is isolated, the proton NMR spectrum of which, in deuterated chloroform, has the following characteristics:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04788204 |
| Source dataset | uspto-grants-1988_11 |
| ORD ID | ord-a72e822aab334b719d775f0c7bc0ef11 |
| Source note | uspto-grants-1988_11 |