Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl formate → N-[3-(Trimethoxysilyl)propyl]formamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl formate | HCID 7865 | — |
| 반응물 | Aminopropyltrimethoxysilane | HCID 83756 | — |
| 생성물 | N-[3-(Trimethoxysilyl)propyl]formamide | HCID 14388644 | — |
반응 단계
A mixture of 7 parts (39 mmol.) of 3-aminopropyltrimethoxysilane and 20 parts (330 mmol.) of methyl formate was heated under reflux in a nitrogen atmosphere. The reaction was monitored by gas chromatography and was found to be complete after 3 hours. Volatiles were then removed in vacuum, yielding the desired N-(3-trimethoxysilylpropyl)formamide.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04788310 |
| 출처 데이터셋 | uspto-grants-1988_11 |
| ORD ID | ord-fb7812a19df8447aa7e6e464e79de421 |
| 출처 메모 | uspto-grants-1988_11 |