HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → HCID 14250821, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Methyl Methacrylate | HCID 6658 | — |
| Reactant | 1,4-Cyclohexanedione | HCID 12511 | — |
| Reactant | Pyrrolidine | HCID 31268 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Toluene | HCID 1140 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 14250821 | HCID 14250821 | — |
Reaction Steps
Using cyclohexane-1,4-dione, pyrrolidine and methyl methacrylate (30.0 g, 0.3 mole), the procedure of Example 2 was repeated except that benzene was used in lieu of toluene and ethanol in lieu of dioxane to give 14.8 g of oil. Using a Kugel vacuum distillator, the oil was treated at an oven temperature of 190°-210° C. (1.0-1.2 mmHg) to give a colorless viscous oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04788315 |
| Source dataset | uspto-grants-1988_11 |
| ORD ID | ord-8fce3a6124414afa99a3307b7e135b90 |
| Source note | uspto-grants-1988_11 |