Sulfuric Acid → HCID 21284041, compound

HRID 2232619Notes

Reaction equation

HRID 2232619 reaction equation
S(=O)(=O)(O)O.[CH3:6][CH:7]([CH:13]1[CH2:18][C:17](=[O:19])[CH:16]([CH:20]([CH3:26])[CH2:21][C:22]([O:24]C)=[O:23])[CH2:15][C:14]1=[O:27])[CH2:8][C:9]([O:11]C)=[O:10]>>[CH3:26][CH:20]([CH:16]1[CH2:15][C:14](=[O:27])[CH:13]([CH:7]([CH3:6])[CH2:8][C:9]([OH:11])=[O:10])[CH2:18][C:17]1=[O:19])[CH2:21][C:22]([OH:24])=[O:23]

Participants

3

Reactant 2

HCID 1118Sulfuric AcidHCID 14250820HCID 14250820, compound

Product 1

HCID 21284041HCID 21284041, compoundYield 87.9%

Procedure

In an aqueous medium in the presence of sulfuric acid as the catalyst, 3.0 g of the oil obtained in Example 4 was hydrolyzed under reflux for 8 hours. The procedure gave 2.4 g of crystals.

Workup

  1. temperatureunder reflux for 8 hours

Sources & evidence

ORD record
ord-fac0da22f1fc4a7a931b05bbf0a77655
Source dataset
uspto-grants-1988_11
Patent number
US04788315

Reaction notes

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