HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → (4-Fluorobenzyl)triphenylphosphonium bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | 3-Fluorobenzyl bromide | HCID 68007 | — |
| Product | (4-Fluorobenzyl)triphenylphosphonium bromide | HCID 10837295 | — |
Reaction Steps
A solution of 3-fluorobenzyl bromide (4.73 g) in dry toluene (5.0 cm3) was added to a stirred suspension of triphenylphosphine (4.87 g) in dry toluene (5.0 cm3) and after 30 minutes the resultant precipitate was collected by filtration and washed with toluene to yield 4-fluorobenzyltriphenylphosphonium bromide (7.1 g) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04788348 |
| Source dataset | uspto-grants-1988_11 |
| ORD ID | ord-9a60d3c50a7f4a1ca002269943efbba9 |
| Source note | uspto-grants-1988_11 |