HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chlorododecane → 3-Dimethylaminopropyl Laurate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chlorododecane | HCID 8192 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 3-(Dimethylamino)-1-propanol | HCID 76646 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 3-Dimethylaminopropyl Laurate | HCID 3613080 | — |
Reaction Steps
In accordance with the procedure of Example 10, 72.2 g of 3-dimethylamino-1-propanol and 153.1 g of lauryl chloride are reacted in altogether 250 ml of CHCl3. The reaction mixture is neutralised with 147 ml of 20% NaOH. Yield: 157.2 g (82.1%) of product with a boiling point of 110° C./0.1 torr.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04352913 |
| Source dataset | uspto-grants-1982_10 |
| ORD ID | ord-46d16faaa6464c50bf3707fe16399824 |
| Source note | uspto-grants-1982_10 |