HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrophenol → HCID 14994114, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrophenol | HCID 980 | — |
| Reactant | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Reactant | HCID 14347260 | HCID 14347260 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 14994114 | HCID 14994114 | 100.5% |
Reaction Steps
As in Example 115, a solution of (E)-5,5-bis [(1,1'-biphenyl)-4-yl]-2,4-pentadienoic acid (0.673 g) and 4-nitrophenol (0.256 g) in dichloromethane (7 mL) was treated with 1,3-dicyclohexylcarbodiimide (0.345 g). The mixture was stirred at room temperature for 1.5 hours. The usual work up furnished 0.88 g of (E)-5,5-bis[(1,1'-biphenyl)-4-yl]-2,4-pentadienoic acid 4-nitrophenyl ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04788206 |
| Source dataset | uspto-grants-1988_11 |
| ORD ID | ord-6e996bf38e0e41a2af1761080e029934 |
| Source note | uspto-grants-1988_11 |